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Nathaniel's papers related to business and to the New York Life Insurance Company. There are also letters from Nathaniel to Samuel during the Civil War years. Letters to Samuel from relatives, including his sisters Effie and Fannie and his mother Jane, contain commentary on the Civil War. At different times during the war Samuel was in New Orleans, Manassas and Petersburg. There are Confederate passes among his papers. There is also an 1865 letter from Samuel to his mother about his return home. Samuel's correspondence from his friend Maurice Hurley mentions that Hurley was exiled to Canada to avoid taking the "oath to President Lincoln" in 1864. Correspondence of Nathalie Boush Asher and her husband G. Gordon Asher make up the remainder of the collection. There is also an 1893 Alexandria Female Institute report card for Nathalie. Most of her correspondence is personal letters, sympathy notes, and some letters on House of Representatives stationary. Her interest in politics is indicated by the latter plus newspapers that she saved relating to the candidacy of C.C. Carlin and E.B. White for the 1918 Virginia Eighth District election for the U.S. House of Representatives. There are several pieces of business and personal correspondence to G. Gordon Asher.

Family papers, letters, wills, and deeds of the Chapman Family of Maryland and Virginia.

This collection contains printed matter such as brochures of George Washington's birthday, the Washington Board of Trade, the Suburban Spectator and others. Additionally, there are limited correspondence, reports of the Historic Alexandria Foundation, annual reports of the Alexandria Library, several booklets, photographs, and postcards.

This collection consists of three series related to the McKnight, Piercy, and Jacobs families. In each series there are sub-series of letters, legal documents, and genealogical materials. Contents also include military records, harbor and ballast master papers, an 1849 inaugural ball invitation, and miniature portraits of William P. McKnight and Margaret Jacobs. McKnight correspondence relates to the Civil War.

The bulk of these papers are correspondence between Robert Rutledge and Harriet Hulfish. Besides information about their relationship, this correspondence refers to Army camp life where Rutledge was stationed in Camp Lee, Virginia; San Francisco, California; Tennessee; Kentucky; and Texas. The papers also contain an illustrated catalog of Staunton Military Academy, and a play and short stories authored by Rutledge.

This collection pertains to the house on 607 Oronoco Street. The Sayers opened the house for Garden Week in Virginia, the Tour of Interiors and the Alexandria Garden Club Tour of Five Estates. Included are the pamphlets for the Tour of Interiors of Historic Homes in Alexandria and Garden Week in Virginia and the registers from the Tour of Historic Homes for the 1934 to 1941 period.

This collection consists of letters, notes, business documents, and genealogical research from and on the Shakes, Carne, and Ficklin families. The materials were donated by various uknown donors from 1983-2015 and compiled into a collection created by Alexandria Library's Lloyd House and later Local History/Special Collections branch.